Glycosciences.DB structure entry #375:

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 2D Structure
b-D-Galp-(1-3)-D-GalNAc-ol
 SNFG-style Graphics
  3D Structure Model
 General Structure Data
 Composition
  NMR Proton Chemical Shift Info

MHz 500
Temperature 300
Solvent D2O
Note a)From Eur J Biochem (1981) 118: 487-495, at 360 MHz.
Residue Linkage Proton PPM JFrom JTo Hz Note
D-GalNAc-ol    H1  3.810      0  a
D-GalNAc-ol    H1'  3.730      0  a
D-GalNAc-ol    H2  4.392      0  
D-GalNAc-ol    H3  4.064      0  
D-GalNAc-ol    H4  3.507      0  
D-GalNAc-ol    H5  4.194      0  
D-GalNAc-ol    H6  3.690      0  a
D-GalNAc-ol    H6'  3.650      0  a
D-GalNAc-ol    NAC  2.051      0  
b-D-Galp  3  H1  4.477      0  
b-D-Galp  3  H2  3.564      0  a
b-D-Galp  3  H3  3.754      0  a
b-D-Galp  3  H4  3.901      0  
MHz 500
Temperature 300
Spectrometer Bruker AMX 500
Residue Linkage Proton PPM JFrom JTo Hz Note
D-GALNAC-OL    H2  4.392        note
D-GALNAC-OL    H3  4.063        note
D-GALNAC-OL    H4  3.508        note
D-GALNAC-OL    H5  4.195        note
D-GALNAC-OL    NAc  2.050        note
B-D-GALP  3  H1  4.477        note
B-D-GALP  3  H2  3.564        note
B-D-GALP  3  H4  3.901        note
  NMR Carbon Chemical Shift Info

MHz 0
Temperature 0
Solvent D2O
Residue Linkage Carbon PPM JFrom JTo Hz Note
D-GalNAc-ol    C1  61.20      0  
D-GalNAc-ol    C2  52.00      0  
D-GalNAc-ol    C3  77.00      0  
D-GalNAc-ol    C4  69.90      0  
D-GalNAc-ol    C5  69.80      0  
D-GalNAc-ol    C6  63.50      0  
b-D-Galp  3  C1  104.40      0  
b-D-Galp  3  C2  71.70      0  
b-D-Galp  3  C3  73.10      0  
b-D-Galp  3  C4  69.10      0  
b-D-Galp  3  C5  75.60      0  
b-D-Galp  3  C6  61.60      0  
  Literature references: 42
 Taxonomy: 8
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